|Table of Contents|

Preparation of Magnetic Core-Shell Fe3O4/Ag Nanoparticles

《南京师大学报(自然科学版)》[ISSN:1001-4616/CN:32-1239/N]

Issue:
2013年04期
Page:
78-
Research Field:
化学
Publishing date:

Info

Title:
Preparation of Magnetic Core-Shell Fe3O4/Ag Nanoparticles
Author(s):
Li Liangliang1Jiang Caiyun2Xu Yongcai2Wang Yuping1Peng Panying1
(1.School of Chemistry and Materials Science,Nanjing Normal University,Nanjing 210097,China) (2.Department of Engineering and Technology,Jiangsu Institute of Economic and Trade Technology, Jiangsu Engineering and Research Center of Food Safety,Nanjing 210
Keywords:
magneticnanoparticleFe3O4Agcore-shell
PACS:
O646
DOI:
-
Abstract:
We prepared Fe3O4 magnetic nanoparticles with core size of 10nm by water co-precipitation.Then we obtained the Fe3O4/Ag nanoparticles with core-shell structure by reducing Ag[(NH3)2]+ with gallic acid as reducer and surface modifier.On the preparation conditions study,the ratio of materials,pH of the solution,crystallization temperature and the amount of sliver nitrate which contributed to the Fe3O4 nanoparticles have been discussed.

References:

[1] Zhang J,Post M,Veres T,et al.Laser-assisted synthesis of superparamagnetic Fe@Au core-shell nanoparticles[J].J Phys Chem B,2006,110(14):7 122-7 128.
[2]Lu A H,Salabs E L,Schüth F.Magnetic nanoparticles:synthesis,protection,functionalization,and application[J].Angewandte Chemie International Edition,2007,46(8):1 222-1 244.
[3]孙涛,王光辉,陆安慧,等.磁性氧化铁纳米颗粒的研究进展[J].化工进展,2010,29(7):1 241-1 250.
[4]陈亭汝,孙瑾.Fe3O4磁性纳米粒子的共沉淀法制备研究[J].应用化工,2009,38(2):226-228.
[5]Hyeon T,Lee S S,Park J,et al.Synthesis of highly crystalline and monodisperse maghemite nanocrystallites without a size-selection process[J].J Amer Chem Soc,2001,123(51):847-856.
[6]Lee Y J,Lee J W,Bae C J,et al.Large-scale synthesis of uniform and crystalline magnetite nanoparticles using reverse micelles as nanoreactors under reflux conditions[J].Adv Mater,2005,15:503-509.
[7]Xu J,Yang H B,Fu W Y.Preparation and magnetic properties of magnetic nanoparticles by sol-gel method[J].J Magn Magn Mater,2007,309(2):307-311.
[8]李剑玲,李德才,张少兰,等.纳米Fe3O4颗粒磁性的影响因素分析[J].科学通报,2010,55(27/28):2 753-2 760.
[9]于文广,张同来,乔小晶,等.不同形貌Fe3O4纳米粒子的氧化沉淀法制备和表征[J].无机化学学报,2006,22(7):1 263-1 268.
[10]周洁,马明,张宇,等.溶胶-凝胶法制备不同尺寸的Fe3O4磁性颗粒及表征[J].东南大学学报:自然科学版,2005,35(4):614-617.
[11]Mizutani N,Iwasaki T,Watano S,et al.Effect of ferrous/ferric ions molar ratio on reaction mechanism for hydrothermal synthesis of magnetite nanoparticles[J].Bull Mater Sci,2008,31(5):713-717.
[12]胡大为,王燕民.合成四氧化三铁纳米粒子形貌的调控机理和方法[J].硅酸盐学报,2008,36(10):1 488-1 493.
[13]崔升,沈晓冬,林本兰.共沉淀法制备纳米Fe3O4影响因素的研究[J].硅酸盐通报,2006,25(3):48-52.
[14]Dai J T,Du Y K,Yang P.Preparation and characterization of Pt/Co-Core Au-Shell magnetic nanoparticles[J].Z Anorg Allg Chem,2006,632(6):1 108-1 111.
[15]Sakai H,Kanda T,Shibata H,et al.Preparation of highly dispersed Core/Shell-type titania nanocapsules containing a single Ag nanoparticle[J].J Am Chem Soc,2006,128(15):4 944-4 945.
[16]Xu Z C,Hou Y L,Sun S H.Magnetic Core/Shell Fe3O4/Au and Fe3O4/Au/Ag nanoparticles with tunable plasmonic properties[J].J Am Chem Soc,2007,129(28):8 698-8 699.
[17]杨晓峰,董相廷,周艳慧,等.贵金属核壳纳米粒子最新研究进展[J].稀有金属材料与工程,2009,38(2):368-372.
[18]黄玉萍,徐淑坤,王文星,等.纳米金催化没食子酸还原法制备纳米银及机理研究[J].无机化学学报,2007,23(10):1 683-1 688.
[19]Yoosaf K,Ipe B I,Suresh C H,et al.In Situ synthesis of metal nanoparticles and selective naked-eye detection of lead ions from aqueous media[J].J Phys Chem C,2007,111(34):12 839-12 847.
[20]Mulvaney P.Surface plasmon spectroscopy of nanosized metal particles[J].Langmuir,1996,12(3):788-800.
[21]Zhang Y X,Ding H L,Liu Y Y,et al.Facile one-step synthesis of plasmonic/magnetic core/shell nanostructures and their multifunctionality[J].J Mater Chem,2012,22:10 779-10 786.

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Last Update: 2013-12-30