[1]李人宇,等.室温固相反应一步合成N-(4-羟基-3-甲氧基苯基亚甲基)-对甲苯胺[J].南京师大学报(自然科学版),2009,32(04):65-67.
　Li Renyu,Li Yongmei,Yang Xujie,et al.One Step Synthesis of N-(4-hydroxy-3-methoxyphenylmethylene)-p-methylaniline by Solid Phase Reaction at Room Temperature[J].Journal of Nanjing Normal University(Natural Science Edition),2009,32(04):65-67.
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室温固相反应一步合成N-(4-羟基-3-甲氧基苯基亚甲基)-对甲苯胺()
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《南京师大学报（自然科学版）》[ISSN:1001-4616/CN:32-1239/N]

卷:
第32卷
期数:
2009年04期
页码:
65-67
栏目:
化学
出版日期:
2009-12-30

文章信息/Info

Title:
One Step Synthesis of N-(4-hydroxy-3-methoxyphenylmethylene)-p-methylaniline by Solid Phase Reaction at Room Temperature
作者:
李人宇1;  2;  李咏梅3;  杨绪杰2;  陆路德2;  汪 信2
1. 连云港师范高等专科学校, 江苏连云港222006 
 2. 南京理工大学材料化学实验室, 江苏南京210094
3. 淮海工学院化工系, 江苏连云港222005
Author(s):
Li Renyu1; 2; Li Yongmei3; Yang Xujie2; Lu Lude2; Wang Xin2
1.Lianyungang Teaching College,Lianyungang 222006,China
关键词:
N-( 4-羟基-3-甲氧基苯基亚甲基)-对甲苯胺;  Schiff碱;  室温固相反应;  表征
Keywords:
N-( 4-hydroxy-3-m ethoxypheny lme thy lene)-p-m ethy lan iline;  schiff base;  so lid phase reaction a t room temperature; cha racte rization
分类号:
TQ246.31
摘要:
以对甲苯胺和香草醛为原料,通过室温固相反应一步合成Schiff碱N-(4-羟基-3-甲氧基苯基亚甲基)-对甲苯胺(C15H15NO2),反应在15 min内完成,产率92%,分别用元素分析、X射线粉末衍射谱、红外光谱和核磁共振氢谱对产物进行了表征.
Abstract:
N-( 4-hydroxy-3-m ethoxypheny lm ethy lene)-p-m ethy lan iline ( C15H15NO2 ) w as synthes ized by the one step so-l id phase reaction o fp-m e thy laniline w ith van illin at room temperature w ithou t so lvent. The reaction was comp leted in 15 m in and the y ie ld w as 92%. The product w as character ized by e lementa l analysis, X- ray powder d iffraction, IR and 1H NMR.

参考文献/References:

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备注/Memo

备注/Memo:
基金项目: 连云港市科技项目( SH 0816)资助.
通讯联系人: 李人宇, 博士, 副教授, 研究方向: 有机化学. E-m a il: lirenyu518@ 163. com.
更新日期/Last Update: 2013-04-23