[1]伊纪峰,朱建一,韩晓磊,等.HS-SPME-GC/MS联用检测红毛菜中的挥发性成分[J].南京师大学报(自然科学版),2009,32(02):103-107.
 Yi Jifeng,Zhu Jianyi,Han Xiaolei,et al.Analysis of Volatile Organic Compounds From Bangia by HS-SPME-GC/MS[J].Journal of Nanjing Normal University(Natural Science Edition),2009,32(02):103-107.
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HS-SPME-GC/MS联用检测红毛菜中的挥发性成分()
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《南京师大学报(自然科学版)》[ISSN:1001-4616/CN:32-1239/N]

卷:
第32卷
期数:
2009年02期
页码:
103-107
栏目:
生命科学
出版日期:
2009-06-30

文章信息/Info

Title:
Analysis of Volatile Organic Compounds From Bangia by HS-SPME-GC/MS
作者:
伊纪峰1 朱建一2 韩晓磊2 许 璞2 余多慰1
1. 南京师范大学生命科学学院, 江苏南京210046
 2. 常熟理工学院生物与食品工程学院, 江苏常熟215500
Author(s):
Yi Jifeng1Zhu Jianyi2Han Xiaolei2Xu Pu2Yu Duowei1
1.School of Life Sciences,Nanjing Normal University,Nanjing 210046,China
关键词:
红毛菜 挥发性成分 HS-SPME-GC /MS
Keywords:
B ang ia vo la tile o rganic com pounds HS-SPM E-GC /MS
分类号:
R284
摘要:
选用PDMS/DVB SPME萃取头,与气相色谱-质谱联用,对萃取温度、萃取时间等参数进行优化,分析了红毛菜的挥发性成分.共分离检测出36种挥发性成分,占总峰面积的97.70%,其中8-十七碳烯(30.76%)与十七碳烷(20.20%)是相对含量最高的成份;其他含量较高的成分分别是醇类(11.12%)、醛类(9.90%)、酯类(6.91%).结果表明:8-十七碳烯与十七碳烷是红毛菜属藻类特征性挥发成分.
Abstract:
H ead space so lid phase m icroex traction coupled w ith g as chrom atography-m ass spectrom etry (H S-SPME-GCM S) w as used to analyse the vo la tile organ ic com pounds ( VOCs) from Bang ia. Thirty-six vo latile compounds we re identified. These constituents represented 97170% o f the tota l peak areas. 8-H eptadecene ( 30176% ) and heptadecane ( 201 20% ) w ere them a jor com ponents wh ich probablyw ere the character isticVOCs, othe r r icher com pounds were alcohol( 11112% ) , a ldehyde ( 91 90% ) and ester( 61 91% ).

参考文献/References:

[ 1] 施之新, 谢树莲, 华栋. 中国淡水藻志: 红藻门# 褐藻门(第十三卷) [M ]. 北京: 科学出版社, 2006: 1-30.
[ 2] M u llerK M, Co leK M, Sheath R G. System atics of Bang ia ( B ang ia les, Rhodophy ta) in No rth Ame rica Ò . B iogeographictrends in karyo logy: chrom osom e num bers and linkage w ith g ene sequence phy logenetic trees [ J] . Bangia Phyco log ia, 2003,42( 3): 209-219.
[ 3] 曾呈奎. 曾呈奎文选(上) [M ]. 北京: 海洋出版社, 1994: 108-116.
[ 4] W oo lco tt G W, K ing R J. Porphyra and Bangia ( bang iaceae, Rhodophy ta) in w arm temperate w ater of eastern Austra lia:
m orpho log ical and mo lecu lar analyses [ J] . Phy co log ical Research, 1998, 46( 2): 111-123.
[ 5] Broom J E S, Farr T J, Ne lsonW A. Phylogeny o f theBang ia flora of New Zea land suggests a southern or ig in fo rPorp hyra
and Bang ia ( bang iaceae, Rhodophyta) [ J]. Mo lecu la r Phy logenetics and Evo lution, 2004, 31( 3): 1197-1207.
[ 6] 孙爱淑, 曾呈奎. 中国红毛菜繁殖方式和染色体研究[ J]. 海洋与湖沼, 1998, 29( 3): 269-273.
[ 7] 马家海, 李水军, 纪焕红, 等. 红毛菜氨基酸和脂肪酸分析[ J]. 中国海洋药物, 2002, 89( 5): 40-42.
[ 8] 刘源, 周光宏, 徐幸莲. 固相微萃取及其在食品分析中的应用[ J] . 食品与发酵工业, 2003, 29( 7): 83-87.
[ 9] 赵钰玲, 李菊白, 戚欢阳, 等. 顶空固相微萃取-气相色谱-质谱联用快速分析八角茴香中风味物质[ J]. 分析实验室,2006, 25( 9): 22-26.
[ 10] Ka jiw araT, Kodam aK, M atsu iK, e t a .l Vo latiel com pounds from Japanesem arine brown a lg ae[ C] / / Teran ish iR, Buttery
G, Sug isaw a H. B ioactive vo la tile com pounds from plants. W ash ing ton DC: Am erican Chem istry Soc ie ty, 1993, 525:103-120.
[ 11] 陈婉珠, 芮汉明, 张玲. 海带腥味物质的H S-SPME-GC-MS分析[ J] . 食品工业科技, 2006, 27( 12): 71-73.
[ 12] AkakabeY, Iw am oto S, M iyam ura S, et a .l Induc tion o f ( Z)-8-heptadecene in m ar ine g reen a lg aBry op sism ax im a by m echanical
wounding [ J] . F isher ies Sc ience, 2007, 73( 5): 1057-1060.
[ 13] Noorderm eerM A, D ijken A JHV, Sm eekens SCM, et a.l Cha racte rization of three c loned and expressed 13-hydrope rox idelyase
isoenzym es from a lfa lfa w ith unusual N-term ina l sequences and d iffe rent enzym e k inetics [ J]. FEBS Lett, 2000, 267( 9): 2473-2482.
[ 14] 赵凌, 沈文飚, 翟虎渠, 等. 植物的脂氢过氧化物酶[ J]. 植物生理学通讯, 2004, 40( 2): 135-140
[ 15] Kajiw ara T, M atsu iK, H atanka A, et a.l D istr ibu tion of an enzyme system producing seaweed flavo r: conv ers ion of fa tty
ac ids to long- chain aldehydes in seaw eeds [ J] . Journa l o f Applied Phyco logy, 1993, 5( 2): 225-230.
[ 16] Boonprab K, M atsui K, Akakabe Y, et a.l Fo rm ation of aldehyde flavor ( n-hexana ,l 3Z-nonena l and 2E-nonenal) in thebrown a lga, Lam inar ia angustata [ J]. Journal o fApplied Phyco logy, 2006, 18( 3): 409-412.
[ 17] Kangsadan B, K en jiM, Yo shih ikoA, et a.l H ydrope roxy-arach idon ic ac id m ediated n-hexana l and ( Z)-3-and ( E)-2-nonenal form a tion in Lam inaria angusta ta [ J]. Phy tochem istry, 2003, 63( 6): 669-678.

备注/Memo

备注/Memo:
基金项目: 国家自然科学基金( 30740042)资助项目.
通讯联系人: 余多慰, 博士, 教授, 研究方向: 结构分子生物学. E-m ail:yuduow e@i n jnu. edu. cn
更新日期/Last Update: 2013-04-23